PURE EHO CARTS WITH JAR TECH DECARB

To avoid the mystery hotdog water that makes up a good portion of the retail vape cartridge market people are increasingly very interested in making their own clean carts to control exactly what’s in them for their health and safety and make the best use of the cannabis they have.  The process has been hard to decipher, leading to poor results in most cases and people giving.  I’m here to change that.

This post will provide a very easy path forward to make clean, very potent, and the highest-quality pure full spectrum oil vape carts using straight Ethanol Honey Oil (EHO) made with a Source Turbo or EtOH PRO ethanol recovery device by ExtractCraft (https://www.extractcraft.com).

PROBLEMS NO MORE

Two primary factors that have made making high-quality carts illusive for the home crafter.  First, old style wicked carts require the EHO to be thin enough to soak into the wick so excessive cutting additives must be added.  Ceramic coil “CCell” carts have changed that and now straight EHO concentrate or distillate can be used with no problem, and no need for adjusting viscosity.  Terpenes can still be added for flavor or effect but it’s no longer a requirement.  The second problem comes from the tendency of THC-A from high quality material “crashing” or crystallizing once loaded.  There are two ways to stop crashing; the concentrate can be substantially diluted with additives and/or the EHO can be partially decarbed.  Unfortunately, for the home user both solutions have not really led to quality cart making.  Dilution makes the carts less potent and increases harshness while traditional decarb techniques completely ruin the EHO’s flavor and substantially oxidize the end product.  Come to find out, we have been over complicating this for a long time.  By using a simple jar tech for partial decarb we can make incredible, pure, full spec EHO carts with potency up to +/- 85% quite easily.  I’m going to show you how right now!

HIGH-QUALITY EHO CARTS

STEP 1: MAKE CLEAN EHO 

For this demonstration I used very high-quality flower that was nicely cured, broke the nugs a little causing as little damage as possible and put the cannabis and ethanol separately on dry ice in a cooler overnight.  When temps at -50°F I performed a 1-hour wash, agitating every 15-minutes, filtered well with a Buchner funnel, processed using the EtOH PRO by Extractcraft, and stopped the process while the contents were still very loose.

Loose pour directly from EtOH PRO

NOTE: I always use only food-grade, non-denatured ethanol and recommend everyone else working with extraction in a home environment does as well.

*If you are unfamiliar with the ethanol extraction process above there are some other posts on this site that will help and the ExtractCraft equipment can be found on http://www.extractcraft.com

Cannabis Alcohol Extraction at Home: Process & Equipment

Ethanol Extraction: Complete Breakdown

Super-Cooled QWET Wash for Cannabis Extraction Using Dry Ice

STEP 2: PURGE

I stopped the EtOH PRO process a little early for maximum control so it required a little added purging attention.  The thin oil set over night to thicken a little before going into my vacuum oven for further post process purging.  A vacuum oven works really well but you can also use other methods like the purge mode with aux vac lid on the EtOH PRO, a regular vac chamber with a heating pad, or just take more time to allow natural evaporation and purging.  

Many people get obsessively focused on the amount of residual ethanol in the end product.  The funny part is they never know why they are worried in meaningful terms, or what concentration they would consider to be ok.  The facts are pretty simple, there are no known adverse health effects I can find published anywhere for residual ethanol in the minute concentrations we’re dealing with when consumed orally or by vaping.  If you are concerned, this is what I suggest; do some research to find what level of residual ethanol you are comfortable with, purge accordingly, and have the extraction lab tested before proceeding.  Personally, I’m frankly not worried about minute food grade ethanol residuals at all and purge using an experienced eye to get it low enough to establish stability and eliminate an ethanol flavor but not heavy enough to over purge and negatively affect terpenes.  

STEP 3: JAR TECH PARTIAL DECARB

This is where my game completely changed.  Traditional decarb destroys flavor and terpenes and CWD (Closed Wash Decarb link) is a bit beyond most people’s abilities, leaving no viable high-quality path forward for the home crafter…….until now.  Jar tech has been used with hydrocarbon extractions for crashing and making diamonds for a while and more recently with rosin as well.  I was getting frustrated trying unsuccessfully to apply the process to ethanol extraction when it hit me.  Just use jar tech for partial decarb to make great carts! I’m really excited because this just really opened the door for us and the quality is far better than any cart I’ve ever made.

JAR TECH PARTIAL DECARB PROCESS:

1) Fill a small 2oz canning jar with 10g-20g of EHO. 

2) Place jar in pre-heated oven, souse vide, Instant Pot, or whatever works best that can maintain semi-even heat.  I believe a heating pad can work as well with a longer ramp time added but I haven’t tested it yet.

3) Heat for the prescribed time.

4) Allow it to cool. 

5) Load into warmed glass syringe when at a temp that can be handled safely.

(Excessive ethanol heated in a jar can become dangerous so a safe degree of purging of the extraction in necessary before doing jar tech)

I don’t have reliable access to testing and this is fairly new so I’m still working on nailing this process down.  I’ve performed the process four times so far and it appears to be pretty robust.  Both of the following temp/time combinations seem to work well: 180°F for 3-hours and 225°F for 40-min.  The 225°F for 40-min was used in this exercise.  I think the lower temp for longer works better in most cases but the faster higher temp method worked great here as you can see from the results.  I may adjust this time/temp section as I work with it more.

JAR TECH ADDITIONAL NOTES:

A trick used in rosin jar tech to create positive pressure in the jar is to cool the jar and contents without being sealed, then seal it and add heat.  As heating builds, the pressure in the jar will increase, helping achieve separation when trying to get THC-A to crash.  I believe this may also aid in our quest to maintain as many terps as possible during decarb.  The closed environment with positive pressure hopefully restricts the terps from trying to evaporate.  Obviously, exercise reasonable caution when dealing with drastic temp differences and glass jars.

There was an unexpected surprise after letting this jar cool to 100°F and getting it ready to load into the glass syringe.  It appears the positive pressure in the jar restricted the CO2 bubbles breaking off during decarb and only released once the positive pressure was removed and was stirred.  

One moment everything normal, then CO2 release…….surprise!

This bubble release didn’t happen the other three times I worked with this process so I’m not sure why it happened here.  As surprising and cool as it was, it wasn’t a problem at all.  After allowing it to settle for a couple hours at 90°F it returned from foam to normal EHO.  The reason I gave it a stir is because you may see some separation with a terpene layer on top, so to evenly distribute you many need to gently stir before loading.

This same jar tech can be used for a longer period to achieve full decarb for edibles as well.  The one time I’ve done this I heated for an hour at 220°F and then left at 180°F overnight, then allowed it to cool completely before opening.  I wasn’t able to have it lab tested, but after licking the spoon I’m pretty sure it was fully converted, wonderfully terpy and made the best tincture concentrate I’ve ever had.

STEP 4: FILL CARTS

A 10 ml glass syringe with 14 gauge Luer-Lock blunt tips works well for small batches.  The 14 gauge tip barely fits into the CCells I’m using but the flow is so good it’s worth wrestling with a little.  Make sure to confirm the tips you’re using fit into the carts before starting.  Filling a slightly warmed syringe from the top with warmed EHO and moving quickly allows you to manhandle the EHO through the syringe without much trouble.  I used to try to suck oil up through the needle then fill a cart or two at a time and it never worked well, filling from the top and doing all at once works much better for me.  If you have trouble with the syringe flow you can always hit very lightly with a little heat.

STEP 5: CAP AND START PUFFING

STEP 6: RECOVER WHAT YOU LOST

The two downsides to making your own high-quality carts are transfer loss and low yields.  Luckily, both of these are completely recoverable getting very close to 100% efficiency of material use.

Transfer Loss:

When making carts the EHO moves around a lot.  It comes out of the EtOH PRO or Source Turbo, onto a mat, into a jar, into a glass syringe and into carts.  With so many large contact surfaces and utensils used along the way, there’s a good amount of oil that gets left behind in transfer.  Oil on easy to reach surfaces like mats and such can be collected with dab tools once it dries a bit, but jars and syringes make it more difficult.  Use a little ethanol to break down the oil stuck on the jar and soak the syringe parts in a Ziplock bag with as little ethanol as possible to cover surfaces.  The ethanol used to break down and collect the oil can be run through the Source Turbo, air dried, or saved to run in the next batch.  There should be no loss in the end.

Yield Recovery:

Quality and yield end up representing opposing forces in every type of extraction.  If you aren’t familiar with why that is I’m not going to get into it here, but if you are interested you can find the information in the post EXTRACTION AND YIELD: IT’S A BALANCE.  Any yield left behind in the starting material can be picked up by running it a second time and bringing the total pick-up efficiency to nearly 100%.

APENDIX: ADDING TERPENES 

This post was specifically about making pure EHO carts so I excluded guidance on the addition of terpenes. Even though they aren’t “necessary,” I do like to add terps to my carts and encourage people to experiment with them because it’s fun and can add new dimensions to carts always made with the same material and become boring.  You can either mix terps into the jar just before loading the syringe, or you can just put a drop or two in a cart after filling and before capping.  

Adding to the top of the cart isn’t really the best approach, but it works pretty well. What it lacks in proper process it makes up for in flexibility of testing and playing with many profiles in small sample size.

I hope you learned something, I sure did! Thanks for checking out the post.

STAY LIFTED MY FRIENDS !!!

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16 thoughts on “PURE EHO CARTS WITH JAR TECH DECARB

  1. Thank you for sharing this process Troy! Two questions:
    – to achieve positive pressure in the jar, do you cool the jar and EHO in the fridge or is room temperature sufficient?
    -what time/temp would you recommend using jar tech if you want to fully decarb (eg for edibles)? I’ve been doing CWD 150F for 3 days (sous vide) prior to using the source and it gives my gummies a nice depth of flavour with the terpenes preserved. But if there’s a temp at which terpenes are still preserved that takes less than 3 days, that would be fantastic.

    1. Who is Troy? I put in freezer for about 10 min. Temp and time is hard to say for sure as I haven’t had a chance to test. I’d assume it’s pretty much the same temp scale as other methods. Maybe 220F for 90-min + ramp?

  2. im wondering if this technique can be used after a full purge in a vac oven. After my wash and purge im left with a 8ram hockey puck of oil, Its quite stable. Did i take it too far already for this technique? As it stands i cant see this working in my my c-cells as its i feel its just too hard (even after warming it up it for my syringe )- wont it just get real hard again and not be viscous enough after i fill the carts, or will this decarb method permanently change the viscosity? TIA!!

    1. 1) decarb makes it slightly less viscous. 2) the heat will make it easier to get in a cart 3) you have to move expeditiously 4) use the largest tip you can 5) keep syringe warm

  3. Preference of glass syringe? The interwebs are flooded with them and none seem to be that great.

      1. put shatter in the hdpe bottle
        decarb 180F over night
        if oil seperates into 2 layers, mix them
        let it cool
        now i should have ready decarbed oil
        every time i would want to refill cart, i would heat bottle (150F maybe more), put tip in cart, and squeeze gently if needed.

        I would use bottle that has a tip slim enough to fit in a cartridge.
        (like this one but 10ml instead of 50ml http://www.kefo.rs/dropping-bottlespewith-dropper-tip-can-3). I won’t be able to squeeze out everything but there’s no need to. I’ll reuse bottle anyway.
        To your knowledge, would that work?

      2. I think there is very little chance that will work as well as you may imagine. Heating too much in open air is going to lower quality substantially. Using a glass syringe as mentioned and demonstrated is your best approach

      3. Oil would get degraded even if bottle was air tight while decarbing? I have a cap for bottle and it doesnt leak

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